%0 Journal article
%A Bender, Philipp
%A Honecker, Dirk
%A Bersweiler, Mathias
%A Costo, Rocio
%A Kahmann, Tamara
%A Ludwig, Frank
%A Leiner, Jon
%A Jochum, Johanna K.
%T Robust approaches for model‐free small‐angle scattering data analysis
%R 10.1107/S1600576722004356
%J Journal of Applied Crystallography
%V 55
%N 3

%I International Union of Crystallography
%X The small‐angle neutron scattering data of nanostructured magnetic samples contain information regarding their chemical and magnetic properties. Often, the first step to access characteristic magnetic and structural length scales is a model‐free investigation. However, due to measurement uncertainties and a restricted q range, a direct Fourier transform usually fails and results in ambiguous distributions. To circumvent these problems, different methods have been introduced to derive regularized, more stable correlation functions, with the indirect Fourier transform being the most prominent approach. Here, the indirect Fourier transform is compared with the singular value decomposition and an iterative algorithm. These approaches are used to determine the correlation function from magnetic small‐angle neutron scattering data of a powder sample of iron oxide nanoparticles; it is shown that with all three methods, in principle, the same correlation function can be derived. Each method has certain advantages and disadvantages, and thus the recommendation is to combine these three approaches to obtain robust results.
%U http://resolver.sub.uni-goettingen.de/purl?gldocs-11858/10220
%~  FID GEO-LEO e-docs