%0 Journal article %A Johnston, Andrea %A Florence, Alastair J. %A Fabbiani, Francesca J. A. %A Shankland, Kenneth %A Bedford, Colin T. %A Bardin, Julie %T Cytenamide trifluoroacetic acid solvate %R 10.1107/S1600536808016577 %R 10.23689/fidgeo-2465 %J Acta Crystallographica Section E Structure Reports Online %V 64 %N 7 %X Cytenamide forms a 1:1 solvate with trifluoroacetic acid (systematic name: 5H-dibenzo[a,d]cycloheptatriene-5-carboxamide trifluoroacetic acid solvate), C16H13NO C2HF3O2. The compound crystallizes with one molecule of cytenamide and one of trifluoroacetic acid in the asymmetric unit; these are linked by O—H O and N—H O hydrogen bonds to form an R2 2(8) motif. The trifluoromethyl group of the solvent molecule displays rotational disorder over two sites, with siteoccupancy factors of 0.964 (4) and 0.036 (4). %U http://resolver.sub.uni-goettingen.de/purl?gldocs-11858/6778 %~ FID GEO-LEO e-docs