Novel experimental setup for megahertz X‐ray diffraction in a diamond anvil cell at the High Energy Density (HED) instrument of the European X‐ray Free‐Electron Laser (EuXFEL)
Konôpková, Z.
Appel, K.
Prescher, C.
Schropp, A.
Cerantola, V.
Husband, R. J.
McHardy, J. D.
McMahon, M. I.
McWilliams, R. S.
Pépin, C. M.
Mainberger, J.
Roeper, M.
Berghäuser, A.
Damker, H.
Talkovski, P.
Foese, M.
Kujala, N.
Ball, O. B.
Baron, M. A.
Briggs, R.
Bykov, M.
Bykova, E.
Chantel, J.
Coleman, A. L.
Cynn, H.
Dattelbaum, D.
Dresselhaus-Marais, L. E.
Eggert, J. H.
Ehm, L.
Evans, W. J.
Fiquet, G.
Frost, M.
Glazyrin, K.
Goncharov, A. F.
Hwang, H.
Jenei, Zs.
Kim, J.-Y.
Langenhorst, F.
Lee, Y.
Makita, M.
Marquardt, H.
McBride, E. E.
Merkel, S.
Morard, G.
O'Bannon, E. F.
Otzen, C.
Pace, E. J.
Pelka, A.
Pigott, J. S.
Prakapenka, V. B.
Redmer, R.
Sanchez-Valle, C.
Schoelmerich, M.
Speziale, S.
Spiekermann, G.
Sturtevant, B. T.
Toleikis, S.
Velisavljevic, N.
Wilke, M.
Yoo, C.-S.
Baehtz, C.
Zastrau, U.
Strohm, C.
DOI: https://doi.org/10.23689/fidgeo-4428
Liermann, H. P.; Konôpková, Z.; Appel, K.; Prescher, C.; Schropp, A.; Cerantola, V.; Husband, R. J.; McHardy, J. D.; McMahon, M. I.; McWilliams, R. S.; Pépin, C. M.; Mainberger, J.; Roeper, M.; Berghäuser, A.; Damker, H.; Talkovski, P.; Foese, M.; Kujala, N.; Ball, O. B.; Baron, M. A.; Briggs, R.; Bykov, M.; Bykova, E.; Chantel, J.; Coleman, A. L.; Cynn, H.; Dattelbaum, D.; Dresselhaus-Marais, L. E.; Eggert, J. H.; Ehm, L.; Evans, W. J.; Fiquet, G.; Frost, M.; Glazyrin, K.; Goncharov, A. F.; Hwang, H.; Jenei, Zs.; Kim, J.-Y.; Langenhorst, F.; Lee, Y.; Makita, M.; Marquardt, H.; McBride, E. E.; Merkel, S.; Morard, G.; O'Bannon, E. F.; Otzen, C.; Pace, E. J.; Pelka, A.; Pigott, J. S.; Prakapenka, V. B.; Redmer, R.; Sanchez-Valle, C.; Schoelmerich, M.; Speziale, S.; Spiekermann, G.; Sturtevant, B. T.; Toleikis, S.; Velisavljevic, N.; Wilke, M.; Yoo, C.-S.; Baehtz, C.; Zastrau, U.; Strohm, C., 2021: Novel experimental setup for megahertz X‐ray diffraction in a diamond anvil cell at the High Energy Density (HED) instrument of the European X‐ray Free‐Electron Laser (EuXFEL) . In: Journal of Synchrotron Radiation , 28 , 3 , 688 -706, DOI: https://doi.org/10.23689/fidgeo-4428.
Konôpková, Z.; 2European X-Ray Free-Electron Laser Facility GmbH, Holzkoppel 4, 22869 Schenefeld, Germany
Appel, K.; 2European X-Ray Free-Electron Laser Facility GmbH, Holzkoppel 4, 22869 Schenefeld, Germany
Prescher, C.; 1Photon Sciences, Deutsches Elektronen-Synchrotron (DESY), Notkestraße 85, Hamburg, Germany
Schropp, A.; 1Photon Sciences, Deutsches Elektronen-Synchrotron (DESY), Notkestraße 85, Hamburg, Germany
Cerantola, V.; 2European X-Ray Free-Electron Laser Facility GmbH, Holzkoppel 4, 22869 Schenefeld, Germany
Husband, R. J.; 1Photon Sciences, Deutsches Elektronen-Synchrotron (DESY), Notkestraße 85, Hamburg, Germany
McHardy, J. D.; 3School of Physics and Astronomy, Centre for Science at Extreme Conditions, and SUPA, University of Edinburgh, Peter Guthrie Tait Road, EdinburghEH9 3FD, United Kingdom
McMahon, M. I.; 3School of Physics and Astronomy, Centre for Science at Extreme Conditions, and SUPA, University of Edinburgh, Peter Guthrie Tait Road, EdinburghEH9 3FD, United Kingdom
Pépin, C. M.; 4CEA, DAM, DIF, F-91297 Arpajon, France
Mainberger, J.; 1Photon Sciences, Deutsches Elektronen-Synchrotron (DESY), Notkestraße 85, Hamburg, Germany
Roeper, M.; 1Photon Sciences, Deutsches Elektronen-Synchrotron (DESY), Notkestraße 85, Hamburg, Germany
Berghäuser, A.; 6Helmholtz Zentrum Dresden Rossendorf e.V., 01328 Dresden, Germany
Damker, H.; 1Photon Sciences, Deutsches Elektronen-Synchrotron (DESY), Notkestraße 85, Hamburg, Germany
Talkovski, P.; 1Photon Sciences, Deutsches Elektronen-Synchrotron (DESY), Notkestraße 85, Hamburg, Germany
Foese, M.; 1Photon Sciences, Deutsches Elektronen-Synchrotron (DESY), Notkestraße 85, Hamburg, Germany
Kujala, N.; 2European X-Ray Free-Electron Laser Facility GmbH, Holzkoppel 4, 22869 Schenefeld, Germany
Ball, O. B.; 3School of Physics and Astronomy, Centre for Science at Extreme Conditions, and SUPA, University of Edinburgh, Peter Guthrie Tait Road, EdinburghEH9 3FD, United Kingdom
Baron, M. A.; 7Institut de Minéralogie, de Physique des Matériaux et de Cosmochimie (IMPMC), Sorbonne Université, UMR CNRS 7590, Musée National d'Histoire Naturelle, 4 Place Jussieu, Paris, France
Briggs, R.; 8Lawrence Livermore National Laboratory, 7000 East Avenue, Livermore, CA 94550, USA
Bykov, M.; 9Carnegie Science, Earth and Planets Laboratory, 5241 Broad Branch Road NW, Washington, DC 20015, USA
Bykova, E.; 9Carnegie Science, Earth and Planets Laboratory, 5241 Broad Branch Road NW, Washington, DC 20015, USA
Chantel, J.; 10Université de Lille, CNRS, INRAE, Centrale Lille, UMR 8207 – UMET – Unité Matériaux et Transformations, F-59000 Lille, France
Coleman, A. L.; 8Lawrence Livermore National Laboratory, 7000 East Avenue, Livermore, CA 94550, USA
Cynn, H.; 8Lawrence Livermore National Laboratory, 7000 East Avenue, Livermore, CA 94550, USA
Dattelbaum, D.; 11Los Alamos National Laboratory, Los Alamos, NM 87545, USA
Dresselhaus-Marais, L. E.; 8Lawrence Livermore National Laboratory, 7000 East Avenue, Livermore, CA 94550, USA
Eggert, J. H.; 8Lawrence Livermore National Laboratory, 7000 East Avenue, Livermore, CA 94550, USA
Ehm, L.; 12Mineral Physics Institute, Stony Brook University, Stony Brook, NY 11794, USA
Evans, W. J.; 8Lawrence Livermore National Laboratory, 7000 East Avenue, Livermore, CA 94550, USA
Fiquet, G.; 7Institut de Minéralogie, de Physique des Matériaux et de Cosmochimie (IMPMC), Sorbonne Université, UMR CNRS 7590, Musée National d'Histoire Naturelle, 4 Place Jussieu, Paris, France
Frost, M.; 13SLAC National Accelerator Laboratory, 2575 Sand Hill Road, Menlo Park, CA 94025, USA
Glazyrin, K.; 1Photon Sciences, Deutsches Elektronen-Synchrotron (DESY), Notkestraße 85, Hamburg, Germany
Goncharov, A. F.; 9Carnegie Science, Earth and Planets Laboratory, 5241 Broad Branch Road NW, Washington, DC 20015, USA
Hwang, H.; 14Department of Earth System Sciences, Yonsei University, 50 Yonsei-ro, Seodaemun-gu, Seoul 03722, Republic of Korea
Jenei, Zs.; 8Lawrence Livermore National Laboratory, 7000 East Avenue, Livermore, CA 94550, USA
Kim, J.-Y.; 15Department of Physics, Research Institute for High Pressure, Hanyang University, 222 Wangsimni-ro, Seoul 04763, Republic of Korea
Langenhorst, F.; 16Institute of Geosciences, Friedrich Schiller University Jena, Carl-Zeiss-Promenade 10, 07745 Jena, Germany
Lee, Y.; 14Department of Earth System Sciences, Yonsei University, 50 Yonsei-ro, Seodaemun-gu, Seoul 03722, Republic of Korea
Makita, M.; 2European X-Ray Free-Electron Laser Facility GmbH, Holzkoppel 4, 22869 Schenefeld, Germany
Marquardt, H.; 17Department of Earth Sciences, University of Oxford, South Parks Road, OxfordOX1 3AN, United Kingdom
McBride, E. E.; 13SLAC National Accelerator Laboratory, 2575 Sand Hill Road, Menlo Park, CA 94025, USA
Merkel, S.; 10Université de Lille, CNRS, INRAE, Centrale Lille, UMR 8207 – UMET – Unité Matériaux et Transformations, F-59000 Lille, France
Morard, G.; 7Institut de Minéralogie, de Physique des Matériaux et de Cosmochimie (IMPMC), Sorbonne Université, UMR CNRS 7590, Musée National d'Histoire Naturelle, 4 Place Jussieu, Paris, France
O'Bannon, E. F.; 8Lawrence Livermore National Laboratory, 7000 East Avenue, Livermore, CA 94550, USA
Otzen, C.; 1Photon Sciences, Deutsches Elektronen-Synchrotron (DESY), Notkestraße 85, Hamburg, Germany
Pace, E. J.; 3School of Physics and Astronomy, Centre for Science at Extreme Conditions, and SUPA, University of Edinburgh, Peter Guthrie Tait Road, EdinburghEH9 3FD, United Kingdom
Pelka, A.; 6Helmholtz Zentrum Dresden Rossendorf e.V., 01328 Dresden, Germany
Pigott, J. S.; 11Los Alamos National Laboratory, Los Alamos, NM 87545, USA
Prakapenka, V. B.; 20Center for Advanced Radiation Sources, University of Chicago, Chicago, IL 60637, USA
Redmer, R.; 21Institut für Physik, Universität Rostock, D-18051 Rostock, Germany
Sanchez-Valle, C.; 22Institut für Mineralogie, University of Münster, Münster, Germany
Schoelmerich, M.; 2European X-Ray Free-Electron Laser Facility GmbH, Holzkoppel 4, 22869 Schenefeld, Germany
Speziale, S.; 23GFZ German Research Centre for Geosciences, Telegrafenberg, 14473 Potsdam, Germany
Spiekermann, G.; 24Institut für Geowissenschaften, Universität Potsdam, Karl-Liebknecht-Straße 24-25, 14476 Potsdam, Germany
Sturtevant, B. T.; 11Los Alamos National Laboratory, Los Alamos, NM 87545, USA
Toleikis, S.; 1Photon Sciences, Deutsches Elektronen-Synchrotron (DESY), Notkestraße 85, Hamburg, Germany
Velisavljevic, N.; 8Lawrence Livermore National Laboratory, 7000 East Avenue, Livermore, CA 94550, USA
Wilke, M.; 24Institut für Geowissenschaften, Universität Potsdam, Karl-Liebknecht-Straße 24-25, 14476 Potsdam, Germany
Yoo, C.-S.; 25Department of Chemistry, Institute of Shock Physics, and Materials Science and Engineering, Washington State University, Pullman, WA 99164, USA
Baehtz, C.; 6Helmholtz Zentrum Dresden Rossendorf e.V., 01328 Dresden, Germany
Zastrau, U.; 2European X-Ray Free-Electron Laser Facility GmbH, Holzkoppel 4, 22869 Schenefeld, Germany
Strohm, C.; 1Photon Sciences, Deutsches Elektronen-Synchrotron (DESY), Notkestraße 85, Hamburg, Germany
Appel, K.; 2European X-Ray Free-Electron Laser Facility GmbH, Holzkoppel 4, 22869 Schenefeld, Germany
Prescher, C.; 1Photon Sciences, Deutsches Elektronen-Synchrotron (DESY), Notkestraße 85, Hamburg, Germany
Schropp, A.; 1Photon Sciences, Deutsches Elektronen-Synchrotron (DESY), Notkestraße 85, Hamburg, Germany
Cerantola, V.; 2European X-Ray Free-Electron Laser Facility GmbH, Holzkoppel 4, 22869 Schenefeld, Germany
Husband, R. J.; 1Photon Sciences, Deutsches Elektronen-Synchrotron (DESY), Notkestraße 85, Hamburg, Germany
McHardy, J. D.; 3School of Physics and Astronomy, Centre for Science at Extreme Conditions, and SUPA, University of Edinburgh, Peter Guthrie Tait Road, EdinburghEH9 3FD, United Kingdom
McMahon, M. I.; 3School of Physics and Astronomy, Centre for Science at Extreme Conditions, and SUPA, University of Edinburgh, Peter Guthrie Tait Road, EdinburghEH9 3FD, United Kingdom
Pépin, C. M.; 4CEA, DAM, DIF, F-91297 Arpajon, France
Mainberger, J.; 1Photon Sciences, Deutsches Elektronen-Synchrotron (DESY), Notkestraße 85, Hamburg, Germany
Roeper, M.; 1Photon Sciences, Deutsches Elektronen-Synchrotron (DESY), Notkestraße 85, Hamburg, Germany
Berghäuser, A.; 6Helmholtz Zentrum Dresden Rossendorf e.V., 01328 Dresden, Germany
Damker, H.; 1Photon Sciences, Deutsches Elektronen-Synchrotron (DESY), Notkestraße 85, Hamburg, Germany
Talkovski, P.; 1Photon Sciences, Deutsches Elektronen-Synchrotron (DESY), Notkestraße 85, Hamburg, Germany
Foese, M.; 1Photon Sciences, Deutsches Elektronen-Synchrotron (DESY), Notkestraße 85, Hamburg, Germany
Kujala, N.; 2European X-Ray Free-Electron Laser Facility GmbH, Holzkoppel 4, 22869 Schenefeld, Germany
Ball, O. B.; 3School of Physics and Astronomy, Centre for Science at Extreme Conditions, and SUPA, University of Edinburgh, Peter Guthrie Tait Road, EdinburghEH9 3FD, United Kingdom
Baron, M. A.; 7Institut de Minéralogie, de Physique des Matériaux et de Cosmochimie (IMPMC), Sorbonne Université, UMR CNRS 7590, Musée National d'Histoire Naturelle, 4 Place Jussieu, Paris, France
Briggs, R.; 8Lawrence Livermore National Laboratory, 7000 East Avenue, Livermore, CA 94550, USA
Bykov, M.; 9Carnegie Science, Earth and Planets Laboratory, 5241 Broad Branch Road NW, Washington, DC 20015, USA
Bykova, E.; 9Carnegie Science, Earth and Planets Laboratory, 5241 Broad Branch Road NW, Washington, DC 20015, USA
Chantel, J.; 10Université de Lille, CNRS, INRAE, Centrale Lille, UMR 8207 – UMET – Unité Matériaux et Transformations, F-59000 Lille, France
Coleman, A. L.; 8Lawrence Livermore National Laboratory, 7000 East Avenue, Livermore, CA 94550, USA
Cynn, H.; 8Lawrence Livermore National Laboratory, 7000 East Avenue, Livermore, CA 94550, USA
Dattelbaum, D.; 11Los Alamos National Laboratory, Los Alamos, NM 87545, USA
Dresselhaus-Marais, L. E.; 8Lawrence Livermore National Laboratory, 7000 East Avenue, Livermore, CA 94550, USA
Eggert, J. H.; 8Lawrence Livermore National Laboratory, 7000 East Avenue, Livermore, CA 94550, USA
Ehm, L.; 12Mineral Physics Institute, Stony Brook University, Stony Brook, NY 11794, USA
Evans, W. J.; 8Lawrence Livermore National Laboratory, 7000 East Avenue, Livermore, CA 94550, USA
Fiquet, G.; 7Institut de Minéralogie, de Physique des Matériaux et de Cosmochimie (IMPMC), Sorbonne Université, UMR CNRS 7590, Musée National d'Histoire Naturelle, 4 Place Jussieu, Paris, France
Frost, M.; 13SLAC National Accelerator Laboratory, 2575 Sand Hill Road, Menlo Park, CA 94025, USA
Glazyrin, K.; 1Photon Sciences, Deutsches Elektronen-Synchrotron (DESY), Notkestraße 85, Hamburg, Germany
Goncharov, A. F.; 9Carnegie Science, Earth and Planets Laboratory, 5241 Broad Branch Road NW, Washington, DC 20015, USA
Hwang, H.; 14Department of Earth System Sciences, Yonsei University, 50 Yonsei-ro, Seodaemun-gu, Seoul 03722, Republic of Korea
Jenei, Zs.; 8Lawrence Livermore National Laboratory, 7000 East Avenue, Livermore, CA 94550, USA
Kim, J.-Y.; 15Department of Physics, Research Institute for High Pressure, Hanyang University, 222 Wangsimni-ro, Seoul 04763, Republic of Korea
Langenhorst, F.; 16Institute of Geosciences, Friedrich Schiller University Jena, Carl-Zeiss-Promenade 10, 07745 Jena, Germany
Lee, Y.; 14Department of Earth System Sciences, Yonsei University, 50 Yonsei-ro, Seodaemun-gu, Seoul 03722, Republic of Korea
Makita, M.; 2European X-Ray Free-Electron Laser Facility GmbH, Holzkoppel 4, 22869 Schenefeld, Germany
Marquardt, H.; 17Department of Earth Sciences, University of Oxford, South Parks Road, OxfordOX1 3AN, United Kingdom
McBride, E. E.; 13SLAC National Accelerator Laboratory, 2575 Sand Hill Road, Menlo Park, CA 94025, USA
Merkel, S.; 10Université de Lille, CNRS, INRAE, Centrale Lille, UMR 8207 – UMET – Unité Matériaux et Transformations, F-59000 Lille, France
Morard, G.; 7Institut de Minéralogie, de Physique des Matériaux et de Cosmochimie (IMPMC), Sorbonne Université, UMR CNRS 7590, Musée National d'Histoire Naturelle, 4 Place Jussieu, Paris, France
O'Bannon, E. F.; 8Lawrence Livermore National Laboratory, 7000 East Avenue, Livermore, CA 94550, USA
Otzen, C.; 1Photon Sciences, Deutsches Elektronen-Synchrotron (DESY), Notkestraße 85, Hamburg, Germany
Pace, E. J.; 3School of Physics and Astronomy, Centre for Science at Extreme Conditions, and SUPA, University of Edinburgh, Peter Guthrie Tait Road, EdinburghEH9 3FD, United Kingdom
Pelka, A.; 6Helmholtz Zentrum Dresden Rossendorf e.V., 01328 Dresden, Germany
Pigott, J. S.; 11Los Alamos National Laboratory, Los Alamos, NM 87545, USA
Prakapenka, V. B.; 20Center for Advanced Radiation Sources, University of Chicago, Chicago, IL 60637, USA
Redmer, R.; 21Institut für Physik, Universität Rostock, D-18051 Rostock, Germany
Sanchez-Valle, C.; 22Institut für Mineralogie, University of Münster, Münster, Germany
Schoelmerich, M.; 2European X-Ray Free-Electron Laser Facility GmbH, Holzkoppel 4, 22869 Schenefeld, Germany
Speziale, S.; 23GFZ German Research Centre for Geosciences, Telegrafenberg, 14473 Potsdam, Germany
Spiekermann, G.; 24Institut für Geowissenschaften, Universität Potsdam, Karl-Liebknecht-Straße 24-25, 14476 Potsdam, Germany
Sturtevant, B. T.; 11Los Alamos National Laboratory, Los Alamos, NM 87545, USA
Toleikis, S.; 1Photon Sciences, Deutsches Elektronen-Synchrotron (DESY), Notkestraße 85, Hamburg, Germany
Velisavljevic, N.; 8Lawrence Livermore National Laboratory, 7000 East Avenue, Livermore, CA 94550, USA
Wilke, M.; 24Institut für Geowissenschaften, Universität Potsdam, Karl-Liebknecht-Straße 24-25, 14476 Potsdam, Germany
Yoo, C.-S.; 25Department of Chemistry, Institute of Shock Physics, and Materials Science and Engineering, Washington State University, Pullman, WA 99164, USA
Baehtz, C.; 6Helmholtz Zentrum Dresden Rossendorf e.V., 01328 Dresden, Germany
Zastrau, U.; 2European X-Ray Free-Electron Laser Facility GmbH, Holzkoppel 4, 22869 Schenefeld, Germany
Strohm, C.; 1Photon Sciences, Deutsches Elektronen-Synchrotron (DESY), Notkestraße 85, Hamburg, Germany
Abstract
The high‐precision X‐ray diffraction setup for work with diamond anvil cells (DACs) in interaction chamber 2 (IC2) of the High Energy Density instrument of the European X‐ray Free‐Electron Laser is described. This includes beamline optics, sample positioning and detector systems located in the multipurpose vacuum chamber. Concepts for pump–probe X‐ray diffraction experiments in the DAC are described and their implementation demonstrated during the First User Community Assisted Commissioning experiment. X‐ray heating and diffraction of Bi under pressure, obtained using 20 fs X‐ray pulses at 17.8 keV and 2.2 MHz repetition, is illustrated through splitting of diffraction peaks, and interpreted employing finite element modeling of the sample chamber in the DAC.
The high‐precision X‐ray diffraction (XRD) setup for work with diamond anvil cells (DACs) in Interaction Chamber 2 of the High Energy Density (HED) instrument of the European X‐ray Free‐Electron Laser is described. image
Subjects
diamond anvil cellsX‐ray free‐electron lasers
high‐precision X‐ray diffraction
finite element modeling