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Cytenamide acetic acid solvate

Johnston, Andrea
Florence, Alastair J.
Fabianni, Francesca J. A.
Shankland, Kenneth
Bedford, Colin T.
Journal: Acta Crystallographica Section E Structure Reports Online; 646; 2008; p. o1175 - o1176
DOI: https://doi.org/10.1107/S160053680801550X
Johnston, Andrea; Florence, Alastair J.; Fabianni, Francesca J. A.; Shankland, Kenneth; Bedford, Colin T., 2008: Cytenamide acetic acid solvate. In: Johnston, Andrea; Florence, Alastair J.; Fabianni, Francesca J. A.; Shankland, Kenneth; Bedford, Colin T. (2008): Cytenamide acetic acid solvate - Acta Crystallographica Section E Structure Reports Online, Vol. 64, Nr. 6, p. o1175-o1176, o1175 - o1176, DOI 10.1107/S160053680801550X.
 
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  • Abstract
In the crystal structure of the title compound (systematic name: 5H-dibenzo[a,d]cycloheptatriene-5-carboxamide ethanoic acid solvate), C16H13NO C2H4O2, the cytenamide and solvent molecules form a hydrogen-bonded R2 2(8) dimer motif, which is further connected to form a centrosymmetric double ring motif arrangement. The cycloheptene ring adopts a boat conformation and the dihedral angle between the leastsquares planes through the two aromatic rings is 54.7 (2) .
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