Cytenamide trifluoroacetic acid solvate

Johnston, Andrea
Florence, Alastair J.
Fabbiani, Francesca J. A.
Shankland, Kenneth
Bedford, Colin T.
Bardin, Julie
Journal: Acta Crystallographica Section E Structure Reports Online; 647; 2008; p. o1215 - o1216
DOI: https://doi.org/10.1107/S1600536808016577
Johnston, Andrea; Florence, Alastair J.; Fabbiani, Francesca J. A.; Shankland, Kenneth; Bedford, Colin T.; Bardin, Julie, 2008: Cytenamide trifluoroacetic acid solvate. In: Johnston, Andrea; Florence, Alastair J.; Fabbiani, Francesca J. A.; Shankland, Kenneth; Bedford, Colin T.; Bardin, Julie (2008): Cytenamide trifluoroacetic acid solvate - Acta Crystallographica Section E Structure Reports Online, Vol. 64, Nr. 7, p. o1215-o1216, o1215 - o1216, DOI 10.1107/S1600536808016577.
 
Thumbnail
View/Open
Metadata Export:
Endnote
BibTex
RIS
Cytenamide forms a 1:1 solvate with trifluoroacetic acid (systematic name: 5H-dibenzo[a,d]cycloheptatriene-5-carboxamide trifluoroacetic acid solvate), C16H13NO C2HF3O2. The compound crystallizes with one molecule of cytenamide and one of trifluoroacetic acid in the asymmetric unit; these are linked by O—H O and N—H O hydrogen bonds to form an R2 2(8) motif. The trifluoromethyl group of the solvent molecule displays rotational disorder over two sites, with siteoccupancy factors of 0.964 (4) and 0.036 (4).
Statistik:
View Statistics
Collection