Combined X-ray and neutron single-crystal diffraction in diamond anvil cells

Grzechnik, Andrzej
Meven, Martin
Paulmann, Carsten
Friese, Karen
DOI: https://doi.org/10.1107/S1600576719014201
Grzechnik, Andrzej; Meven, Martin; Paulmann, Carsten; Friese, Karen, 2019: Combined X-ray and neutron single-crystal diffraction in diamond anvil cells. In: Journal of Applied Crystallography, Band 53, 1: 9 - 14, DOI: 10.1107/S1600576719014201.
 
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It is shown that it is possible to perform combined X-ray and neutron single-crystal studies in the same diamond anvil cell (DAC). A modified Merrill–Bassett DAC equipped with an inflatable membrane filled with He gas has been developed. It can be used on laboratory X-ray and synchrotron diffractometers as well as on neutron instruments. The data processing procedures and a joint structural refinement of the high-pressure synchrotron and neutron single-crystal data are presented and discussed for the first time.
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Subjects:
single-crystal X-ray diffraction
single-crystal neutron diffraction
high pressure
diamond anvil cells
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